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The first stage involves the high - temperature ( 700-970 ° C ) annealing under an argon atmosphere ( Po , = 1 kPa ) or under air ; the second stage is an oxygen annealing ( 450 ° C , 102 kPa ) .
The first stage involves the high - temperature ( 700-970 ° C ) annealing under an argon atmosphere ( Po , = 1 kPa ) or under air ; the second stage is an oxygen annealing ( 450 ° C , 102 kPa ) .
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During the subsequent anneal under an oxygen atmosphere , the X - ray diffraction patterns for all sam- ples ... Upon the first annealing stage , particles of samples 1 and 2 conserve the electron diffraction patterns typical of ...
During the subsequent anneal under an oxygen atmosphere , the X - ray diffraction patterns for all sam- ples ... Upon the first annealing stage , particles of samples 1 and 2 conserve the electron diffraction patterns typical of ...
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X - ray diffraction patterns for KOH - BaO2 - Bi2O3 ( K : Ba = 3.3 ) samples annealed at 400 ° C for 2 h . Ba : Bi = ( a ) 1.00 , ( b ) 0.88 ... Evidently , the phase constitution of the reaction product changes during the annealing .
X - ray diffraction patterns for KOH - BaO2 - Bi2O3 ( K : Ba = 3.3 ) samples annealed at 400 ° C for 2 h . Ba : Bi = ( a ) 1.00 , ( b ) 0.88 ... Evidently , the phase constitution of the reaction product changes during the annealing .
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Vol 46 No 10 | 1437 |
Phase Formation during the LowTemperature Synthesis of KBBO Superconductors in KOH Melt | 1448 |
Synthesis and Properties of Inorganic Compounds | 1462 |
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