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Nickel ẞ - diketonates are isolated by vacuum sublimation from mechanically activated mixtures . The conversion of the starting compounds into nickel ẞ - diketonates is 65-80 % . The reaction course , product yield , and some properties ...
Nickel ẞ - diketonates are isolated by vacuum sublimation from mechanically activated mixtures . The conversion of the starting compounds into nickel ẞ - diketonates is 65-80 % . The reaction course , product yield , and some properties ...
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After the reaction mixture is milled for 2.5 h , its IR spectrum is very similar to the spectrum of nickel acetylacetonate [ 17 , 18 ] . Further mechanical treatment causes no noticeable changes in the IR spectrum .
After the reaction mixture is milled for 2.5 h , its IR spectrum is very similar to the spectrum of nickel acetylacetonate [ 17 , 18 ] . Further mechanical treatment causes no noticeable changes in the IR spectrum .
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X - ray powder diffraction patterns from ( a ) NaHFA , ( b , c ) the NiCl2 + 1.8NaHFA mixture after ( b ) milling for 2 h and ( c ) milling for 2 h followed by heating , and ( d ) Ni ( HFA ) 2 ( reaction product ) .
X - ray powder diffraction patterns from ( a ) NaHFA , ( b , c ) the NiCl2 + 1.8NaHFA mixture after ( b ) milling for 2 h and ( c ) milling for 2 h followed by heating , and ( d ) Ni ( HFA ) 2 ( reaction product ) .
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Isomorphism in the NH44K441UO2CO33 System | 7 |
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