Russian Journal of Inorganic Chemistry, Tập 48,Số phát hành 5-8British Library Lending Division with the cooperation of the Royal Society of Chemistry, 2003 |
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Trang 962
... refined by least - squares calculation in the anisotropic approximation for all non - hydrogen atoms . Because of a strong correlation between the parameters of two HDphg + cations ran- domly occupying closely spaced positions , the ...
... refined by least - squares calculation in the anisotropic approximation for all non - hydrogen atoms . Because of a strong correlation between the parameters of two HDphg + cations ran- domly occupying closely spaced positions , the ...
Trang 1009
... refined in anisotropic approximation , and carbon atoms were refined isotropi- cally ( SHELXL93 [ 20 ] ) . The positions of all hydrogen atoms were calculated and refined using the riding model . The final values of R factors were R1 ...
... refined in anisotropic approximation , and carbon atoms were refined isotropi- cally ( SHELXL93 [ 20 ] ) . The positions of all hydrogen atoms were calculated and refined using the riding model . The final values of R factors were R1 ...
Trang 1164
... refined anisotropically . The positions of hydrogen atoms were calculated geometrically and refined by the " rider " model ( U1 = 0.08 Å2 ) . The final values were R1 = 0.0472 , wR2 = 0.1082 , GOOF 0.972 for 1431 reflections with I > 2 ...
... refined anisotropically . The positions of hydrogen atoms were calculated geometrically and refined by the " rider " model ( U1 = 0.08 Å2 ) . The final values were R1 = 0.0472 , wR2 = 0.1082 , GOOF 0.972 for 1431 reflections with I > 2 ...
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Vol 48 No 5 | 622 |
Synthesis and Crystal Structure | 632 |
Synthesis and Study | 642 |
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absorption According acid activation addition analysis angles anion aqueous atoms band bond calculated cations changes characteristics Chem chemical Chemistry cluster cm-¹ complexes composition compounds concentration constants containing coordination Copyright corresponding crystal curves decrease dependence described determined distances distribution effect electron energy existence experimental extraction formation formed function groups H₂O heating higher hydrogen increases Inorganic intensity interaction involved ions Journal Khim lengths ligand lines measured metal method mixture mol/l molecules Moscow Neorg observed obtained oxide oxygen parameters phase Physics position prepared presence properties range ratio reaction REFERENCES refined reflections region respectively Russian salt samples Sciences shift shows signals similar solid solutions solubility solution solvent space group spectra spectrum stability structure studied synthesis Table temperature thermal tion unit values X-ray diffraction