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The structure was further refined by the full - matrix least - squares method in anisotropic approximation . All hydrogen atoms including those of the solvation DMF molecule were located from a difference synthesis .
The structure was further refined by the full - matrix least - squares method in anisotropic approximation . All hydrogen atoms including those of the solvation DMF molecule were located from a difference synthesis .
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The structures were refined in isotropic approximation . At this stage of the structural refinement , corrections for absorption anisotropy were applied . The structures were further refined by the fullmatrix least - squares method in ...
The structures were refined in isotropic approximation . At this stage of the structural refinement , corrections for absorption anisotropy were applied . The structures were further refined by the fullmatrix least - squares method in ...
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The resulting array of 55 structural amplitude modules was employed for refining the superposition atomic structure ... thermal atomic parameters were refined concurrently for the whole reflection array by the leastsquares method .
The resulting array of 55 structural amplitude modules was employed for refining the superposition atomic structure ... thermal atomic parameters were refined concurrently for the whole reflection array by the leastsquares method .
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Vol 41 No 1 | 1 |
Synthesis and Characterization | 7 |
Deviation from Stoichiometry in Mercury Chalcochromite HgCr₂Se4 | 23 |
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absorption according acid addition analysis angles anions aqueous atoms band bismuth bond bridging calculated carbon cations changes Chem chemical Chemistry chloride cm-¹ complexes composition compounds concentration constants containing coordination Copyright corresponding crystal curves decrease dependence determined distances effect electron elements energy equation equilibrium experimental extraction formation frequency function H₂O heating higher hydrogen increase indicates Inorganic interaction ions Journal Khim ligands measured melting metal method mixture mol/l molecules Moscow Neorg observed obtained occur organic oxidation oxygen atoms parameters peak peritectic phase Physics points position possible prepared present properties Publishing range ratio reaction REFERENCES region respectively Russian salts samples Sciences shows similar sodium solid solutions space group spectra spectrum stability structure studied synthesis Table temperature thermal tion Translation unit values vibrations X-ray diffraction